A phase separation method for analyses of fluoroquinones in meats based on ultrasound-assisted salt-induced liquid-liquid microextraction and a new integrated device

doi:10.1016/j.meatsci.2015.03.023

科研成果详情

题名	A phase separation method for analyses of fluoroquinones in meats based on ultrasound-assisted salt-induced liquid-liquid microextraction and a new integrated device
作者	Wang, Huili1; Gao, Ming2; Xu, Youqu 2; Wang, Wenwei 2; Zheng, Lian 2; Dahlgren, Randy A.3; Wang, Xuedong 2
发表日期	2015-08
发表期刊	MEAT SCIENCE 影响因子和分区
语种	英语
原始文献类型	Article
关键词	Sample extraction Antibacterial agent analysis Fluoroquinolones Ultrasound-assisted Salt-induced Liquid-liquid microextraction Meat
其他关键词	TANDEM MASS-SPECTROMETRY ; POLYCYCLIC AROMATIC-HYDROCARBONS ; RESONANCE BIOSENSOR ASSAY ; EMULSIFICATION MICROEXTRACTION ; FLUORESCENCE DETECTION ; RAPID-DETERMINATION ; WATER SAMPLES ; TRACE LEVELS ; CHROMATOGRAPHY ; (FLUORO)QUINOLONES
摘要	Herein, we developed a novel integrated device to perform phase separation based on ultrasound-assisted, salt-induced, liquid-liquid microextraction for determination of five fluoroquinones in meats by HPLC analysis. The novel integrated device consisted of three simple HDPE (high density polyethylene) parts that were used to separate the solvent from the aqueous solution prior to retrieving the extractant The extraction parameters were optimized using the response surface method based on central composite design: 589 mu L of acetone solvent, pH 2.1, 4.1 min extraction time and 3.5 g of Na2SO4. The limits of detection were 0.056-0.64 mu g kg(-1) and recoveries were 87.2-110.6% for the five fluoroquinones in muscle tissue from fish, chicken, pork and beef. This method is easily constructed from inexpensive materials, extraction efficiency is high, and the approach is compatible, with HPLC analysis. Thus, it has excellent prospects for sample pre-treatment and analysis of fluoroquinones in meat samples. (C) 2015 Elsevier Ltd. All rights reserved.
资助项目	National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21377100, 31270548]; Zhejiang Provincial Natural Science FoundationNatural Science Foundation of Zhejiang Province [LY13B070011, LY14B070013]
出版者	ELSEVIER SCI LTD
出版地	OXFORD
ISSN	0309-1740
EISSN	1873-4138
卷号	106 页码:61-68
DOI	10.1016/j.meatsci.2015.03.023
页数	26
WOS类目	Food Science & Technology
WOS研究方向	Food Science & Technology
WOS记录号	WOS:000355050400011
收录类别	SCIE ; PUBMED ; EI ; SCOPUS
EI入藏号	20151600754887
EI主题词	Solvent extraction
URL	查看原文
PubMed ID	25885797
SCOPUSEID	2-s2.0-84927661810
通讯作者地址	[Wang, Xuedong]College of Environmental Sciences and Public Health, Wenzhou Medical University,Wenzhou,325035,China
Scopus学科分类	Food Science
引用统计	被引频次：10[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	https://kms.wmu.edu.cn/handle/3ETUA0LF/5933
专题	检验医学院（生命科学学院、生物学实验教学中心）仁济学院_环境与公共卫生学部
通讯作者	Wang, Xuedong
作者单位	1.College of Life Sciences, Wenzhou Medical University,Wenzhou,325035,China; 2.College of Environmental Sciences and Public Health, Wenzhou Medical University,Wenzhou,325035,China; 3.Department of Land, Air and Water Resources, University of California,Davis,95616,United States
第一作者单位	检验医学院（生命科学学院、生物学实验教学中心）
通讯作者单位	温州医科大学
第一作者的第一单位	检验医学院（生命科学学院、生物学实验教学中心）
推荐引用方式 GB/T 7714	Wang, Huili,Gao, Ming,Xu, Youqu,et al. A phase separation method for analyses of fluoroquinones in meats based on ultrasound-assisted salt-induced liquid-liquid microextraction and a new integrated device[J]. MEAT SCIENCE,2015,106:61-68.
APA	Wang, Huili., Gao, Ming., Xu, Youqu., Wang, Wenwei., Zheng, Lian., ... & Wang, Xuedong. (2015). A phase separation method for analyses of fluoroquinones in meats based on ultrasound-assisted salt-induced liquid-liquid microextraction and a new integrated device. MEAT SCIENCE, 106, 61-68.
MLA	Wang, Huili,et al."A phase separation method for analyses of fluoroquinones in meats based on ultrasound-assisted salt-induced liquid-liquid microextraction and a new integrated device".MEAT SCIENCE 106(2015):61-68.